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Description of Individual Course Units| Course Unit Code | Course Unit Title | Type of Course Unit | Year of Study | Semester | Number of ECTS Credits | | BMB-23-171 | SpecroelectrochemIstry | Elective | 1 | 2 | 6 |
| | Level of Course Unit | | Second Cycle | | Objectives of the Course | | In the field of spectroelectrochemistry (SEC), the combination of type-oriented spectroscopy and reaction-based electrochemistry, a more complete analysis of single and multiple electron transfer processes and redox reactions is generally carried out. Practical considerations and guidelines will be provided within this course, and selected samples containing UV-VIS-NIR and IR absorption spectroscopy as well as electron paramagnetic resonance (EPR) will be presented to demonstrate the potential and applicability of this technique. The aim of this course is to explain the various technical approaches in spectroelectrochemistry and to reveal the benefits of concepts that are increasingly popular for graduate scientists. | | Name of Lecturer(s) | | Doç. Dr. Bahri GÜR | | Learning Outcomes | | 1 | 1- To learn electrochemical determinations, double layer and thermodynamic properties
2- Learn the technique of voltammetry
3- Learn spectroscopic methods based on electrochemical methods and electrochemical methods.
4- Understand the working principles and properties of spectroscopic devices
5- Learn optically permeable spectroelectrochemistry method and types of optically permeable electrodes
6- To learn IR, FT-IR, Raman, Ellipsometry and ATR spectroscopy techniques and applications
7- To learn the interpretation of surface analysis by SEM, TEM, AFM, STM methods
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| | Mode of Delivery | | Daytime Class | | Prerequisites and co-requisities | | | Recommended Optional Programme Components | | | Course Contents | | 1. Electrochemical double layers and thermodynamic properties
2. Double layer theories
3. Spectroelectrochemistry - UV techniques
4. Optically permeable spectroelectrochemistry
5. IR spectroscopy
6. Spectroelectrochemistry-Vibrating Spectroscopy techniques
7. Impedance Methods
8. Raman Spectroscopy
9. Electron Spin Resonance Spectroscopy
| | Weekly Detailed Course Contents | |
| 1 | Introduction to spectroelectrochemistry
| | | | 2 | Electrochemistry, potentiometry, voltammetry techniques | | | | 3 | Electromagnetic spectrum and Its interference, diffraction, transmission, refraction, reflection, scattering, polarization, absorption and emission | | | | 4 | Spectroscopic devices and its components | | | | 5 | Optical permeable spectroelectrochemistry | | | | 6 | Electrode types | | | | 7 | IR, FT-IR, Reflectance and ATR spectroscopy techniques and their applications | | | | 8 | Midterm | | | | 9 | Laser, Ellipsometry applications, Photothermal, Photoacoustic, Raman Spectroscopy techniques | | | | 10 | X-rays and surface analysis | | | | 11 | Scanning Electron Microscopy (SEM) and Field Emission Scanning Electron Microscopy (FESEM) | | | | 12 | Transmission Electron Microscopy (TEM) | | | | 13 | Low Energy Electron Diffraction (LEED), Scanning Tunneling Microscopy (STM) | | | | 14 | Elecrochemical STM (EC-STM) and Atomic Force Microscopy (AFM) | | |
| | Recommended or Required Reading | | 1. Alanyalıoğlu, M., Spektroelektrokimya, Atatürk University, Faculty of Science, Department of Chemistry, 2010
2. Robert J. Gale (auth.), Robert James Gale (eds.)-Spectroelectrochemistry_ Theory and Practice-Springer US (1988)
3. Wolfgang Kaim and Jan Fiedler, Spectroelectrochemistry the best of two worlds, This journal is c The Royal Society of Chemistry 2009.
4. Tia E. Keyes and Robert J. Forster, Spectroelectrochemistry, National Centre for Sensor Research, School of Chemical Sciences, Dublin City University, Dublin 9, Ireland,
| | Planned Learning Activities and Teaching Methods | | | Assessment Methods and Criteria | |
| Midterm Examination | 1 | 15 | | Discussion | 1 | 5 | | Brain Storming | 1 | 20 | | Criticising Paper | 1 | 10 | | Self Study | 1 | 20 | | Individual Study for Mid term Examination | 1 | 30 | | SUM | 100 | |
| Final Examination | 1 | 50 | | Individual Study for Final Examination | 1 | 50 | | SUM | 100 | | Term (or Year) Learning Activities | 50 | | End Of Term (or Year) Learning Activities | 50 | | SUM | 100 |
| | Language of Instruction | | Turkish | | Work Placement(s) | | None |
| | Workload Calculation | |
| Midterm Examination | 1 | 1 | 1 | | Final Examination | 1 | 2 | 2 | | Attending Lectures | 14 | 3 | 42 | | Practice | 5 | 3 | 15 | | Discussion | 7 | 2 | 14 | | Brain Storming | 7 | 2 | 14 | | Criticising Paper | 7 | 3 | 21 | | Self Study | 10 | 2 | 20 | | Individual Study for Mid term Examination | 1 | 16 | 16 | | Individual Study for Final Examination | 1 | 20 | 20 | | Homework | 7 | 2 | 14 | |
| Contribution of Learning Outcomes to Programme Outcomes | | | * Contribution Level : 1 Very low 2 Low 3 Medium 4 High 5 Very High |
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Iğdır University, Iğdır / TURKEY • Tel (pbx): +90 476
226 13 14 • e-mail: info@igdir.edu.tr
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