Iğdır University Lifelong Learning Programme

Description of Individual Course Units

Course Unit Code	Course Unit Title	Type of Course Unit	Year of Study	Semester	Number of ECTS Credits
9900001095	INSTRUMENTAL ANALYSIS	Compulsory	2	4	5

Level of Course Unit

First Cycle

Objectives of the Course

To provide for the students a safe working environment in laboratory in conformity with legislation and analysis methods; To bring for the students the ability to make pre-purification before analysis; improving the student’s ability and knowledge to make and regulate a solution in different units and concentrations; bring to the students the ability to analyze and evaluate the results using enstrumental devices

Name of Lecturer(s)

Learning Outcomes

1	Student acquires the secure working principle of the laboratory
2	Student comprehends the principles of scales and solution preparation
3	Student comprehends the principles of scales and solution preparation
4	Student explains the results of titration using regulated solution.
5	Student comprehends the principles of work of esntruments such as refractometry, polarimetry, colorimetry, penetrometry, spectrofotometry, titration, densimetry
6	Student explains the results

Mode of Delivery

Daytime Class

Prerequisites and co-requisities

None

Recommended Optional Programme Components

None

Course Contents

Personal security measures, general laboratory safety measures, presentation of materials in the laboratory Weighing process, evaporation, distillation, extraction, heating, cooling. Filtration, precipitation, incineration, drying, crystallization, sublimation. Centrifugation, titrimetry, potentiometry. Dilute and concentrated solutions, unsaturated, saturated and over-saturated solutions. Solution preparation and regulation Densimetry and Colorimetry. Refractometry and polarimetry. Mass spectroscopy, NMR, X-ray. IR sepctroscopy, flame photometry, atomic absorption spectroscopy” Absorption spectroscopy Gas chromatography (gas/gas and gas/liquid) and detector kinds Liquid chromatographies (liquid/solid, liquid/liquid, Ion changing, affinity, adsorption, HPLC, gel filtration) and supercritical fluid chromatography. Elektroforez, “Planar chromatography (paper and thin layer chromatography), electrophoresis

Weekly Detailed Course Contents

Week	Theoretical	Practice	Laboratory
1	Personal security measures, general laboratory safety measures, presentation of materials in the laboratory
2	Weighing process, evaporation, distillation, extraction, heating, cooling.
3	Filtration, precipitation, incineration, drying, crystallization, sublimation.
4	Centrifugation, titrimetry, potentiometry.
5	Dilute and concentrated solutions, unsaturated, saturated and over-saturated solutions.
6	Solution preparation and regulation
7	Densimetry and Colorimetry.
8	Midterm Exam
9	Refractometry and polarimetry.
10	Mass spectroscopy, NMR, X-ray.
11	IR sepctroscopy, flame photometry, atomic absorption spectroscopy”
12	Absorption spectroscopy
13	Gas chromatography (gas/gas and gas/liquid) and detector kinds
14	Liquid chromatographies (liquid/solid, liquid/liquid, Ion changing, affinity, adsorption, HPLC, gel filtration) and supercritical fluid chromatography.
15	Elektroforez, “Planar chromatography (paper and thin layer chromatography), electrophoresis
16	Final Exam

Recommended or Required Reading

Kotancılar, H.G., 2011. Laboratuar Teknikleri ve Enstrümental Analiz Uygulama Klavuzu, Ders notu, Erzurum. Gündüz, T., 2002. İnstrumental Analiz (6. Baskı), Ankara Üniversitesi Kimya Bölümü, Gazi Kitabevi Yayınları. Ankara. s:1357. Skoog, D.A., Holler, F.J., Nieman, T.A., 1998. Principles of Instrumental Analiz. (Çeviri Editörü: Kılıç, E., Köseoğlu, F., Yılmaz, H.) (1. Baskı). Bilim Yayıncılık, Ankara. s:849 Yetim, H., Çam, M., 2009. Enstrümental Gıda Analizleri. Erciyes Üniversitesi Yayınları No:175, Kayseri. s:286

Planned Learning Activities and Teaching Methods

Assessment Methods and Criteria

Term (or Year) Learning Activities	Quantity	Weight
Midterm Examination	1	100
SUM		100
End Of Term (or Year) Learning Activities	Quantity	Weight
Final Examination	1	100
SUM		100
Term (or Year) Learning Activities		40
End Of Term (or Year) Learning Activities		60
SUM		100

Language of Instruction

Turkish

Work Placement(s)

None

Workload Calculation

Activities	Number	Time (hours)	Total Work Load (hours)
Midterm Examination	1	1	1
Final Examination	1	2	2
Self Study	14	8	112
Individual Study for Mid term Examination	1	15	15
Individual Study for Final Examination	1	20	20
Homework	1	10	10
TOTAL WORKLOAD (hours)			160

Contribution of Learning Outcomes to Programme Outcomes

	PO 1	PO 2	PO 3	PO 4	PO 5	PO 6	PO 7
LO1					4
LO2
LO3			2
LO4				3
LO5						3
LO6		2

* Contribution Level : 1 Very low 2 Low 3 Medium 4 High 5 Very High